27-06-2023 дата публикации
Номер: CN116337786A
Принадлежит:
The invention relates to the field of chemical detection, in particular to a method for measuring the content of free silicon in a SiC composite material. The determination method comprises the following steps: S1, drawing a standard curve; s2, taking the ground silicon carbide composite material, adding a sodium nitrate solution, nitric acid and hydrofluoric acid, heating, dissolving, cooling, adding an aluminum chloride solution, fixing the volume, and uniformly mixing; s3, standing the solution after volume metering, taking upper clear liquid, diluting, adding an indicator, neutralizing with ammonia water, adding hydrochloric acid and an ammonium molybdate solution, standing, adding a mixture of oxalic acid and sulfuric acid and a reducing agent, diluting with water, and measuring absorbance by taking water as a reference; the reducing agent is ascorbic acid or stannous chloride; and S4, calculating the content of free silicon in the silicon carbide composite material by using the standard ...
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