28-11-2012 дата публикации
Номер: CN102796620A
Принадлежит:
The invention discloses a fixed bed-based continuous catalytic esterification production method. The fixed bed-based continuous catalytic esterification production method comprises the following steps of 1, mixing a raw material and a lower alcohol having a concentration above 99.5%, wherein the raw material is high-acid value waste vegetable and animal oil or a deodorizer distillate which does not contain impurities and has moisture content of 0.05 to 0.5%, 2, merging a mixed material liquid obtained by the step 1 and an acid, heating to a temperature of 50 to 100 DEG C, and carrying out an esterification reaction process by a fixed bed with a highly acidic resin, 3, carrying out on-line neutralization by an alkali solution, 4, carrying out reduced pressure removal of an alcohol and water, and 5, carrying out reduced pressure distillation to obtain a purified low fatty acid ester. The fixed bed-based continuous catalytic esterification production method can reduce a raw material acid value ...
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