13-02-2014 дата публикации
Номер: WO2014025125A1
Принадлежит:
The present invention relates to a method for preparing a lithium metal phosphor oxide, the method comprising the steps of: mixing an iron salt solution and a phosphate solution in a reactor; applying a shearing force to the mixed solution inside the reactor during the mixing step, and thus forming a suspension containing nano-sized iron phosphate precipitate particles; obtaining nano-sized iron phosphate particles from the suspension; and mixing the iron phosphate with a lithium raw material, and firing, wherein the lithium metal phosphor oxide according to the present invention has the formula of LiMn FePO4, where M is selected from the group consisting of Ni, Co, Mn, Cr, Zr, Nb, Cu, V, Ti, Zn, Al, Ga, and Mg, and n is in the range of 0 to 1. According to the present invention, calcination is conducted at a lower temperature compared to other existing methods, thereby reducing processing costs, and the lithium metal phosphor oxide prepared by the method according to the present invention ...
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