08-11-2016 дата публикации
Номер: KR1020160128927A
Принадлежит:
The present invention relates to a process for preparing graphene oxide, which comprises the steps of: conducting reaction of a plate-like graphite material, an acid solution and an oxidizing agent to obtain graphene oxide; separating the reactants of the reaction into graphene oxide and a waste acid solution; recovering the acid solution and oxidizing agent to the separated waste acid solution and recycling them to the step of preparing graphene oxide; and washing the separated graphene oxide to obtain graphene oxide. According to the process for preparing graphene oxide of the present invention, oxidation of graphite is carried out in a continuous reactor using Taylor vortex flow, and thus the reaction mixture in the reactor shows low viscosity. Therefore, it is possible to separate graphene oxide and the waste acid solution without supplying deionized water additionally and to reuse the separated waste acid solution for oxidizing a plate-like graphite material, such as graphite. As a ...
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